Mene ne ƙa'idojin ƙaura da raguwar iskar shaka na abubuwan da ke cikin petroleum coke yayin aikin calcination?

Tsarin ƙaura da canjin yanayi na abubuwan da aka gano kamar sodium (Na), vanadium (V), nickel (Ni), da calcium (Ca) a cikin petroleum coke yayin calcination suna da alaƙa da yanayin zafi, siffofin faruwa, da halayen sinadarai. Takamaiman tsarin sune kamar haka:

1. Hijira da Sauyawar Sodium (Na)

  • Matakan ƙarancin zafin jiki (<1000°C): Sodium galibi yana wanzuwa ne a cikin nau'in gishirin da ba na halitta ba (misali, sodium sulfate, sodium chloride) ko hadaddun halittu, tare da ƙarancin canjin yanayi. Yayin da zafin ke ƙaruwa, yana rikidewa a hankali ya zama iskar gas (misali, Na₂O) ko hydroxides (misali, NaOH).
  • Matakin zafin jiki mai yawa (>1000°C): Sauyin sodium yana ƙaruwa sosai. Abubuwan da aka samar da sulfur da chlorine (misali, Na₂S, NaCl) suna raguwa ko ruɓewa cikin sauƙi a yanayin zafi mai yawa, wanda ke sa sodium ya fita cikin yanayin iskar gas.
  • Abubuwan da ke tasiri: Yanayin calcination (haɓaka iska/ragewa) yana shafar saurin rushewar sodium sosai. A ƙarƙashin yanayin ragewa, sodium yana da yuwuwar ya yi rauni a cikin nau'in sulfide.

2. Hijira da Sauyawar Vanadium (V)

  • Siffofi na faruwa: Vanadium a cikin petroleum coke galibi yana samuwa ne a cikin siffofi masu ɗaure da sinadarai (misali, vanadyl porphyrins) da siffofi masu karko (misali, vanadium oxides, silicates).
  • Matakan ƙarancin zafin jiki (<1100°C): Vanadium mai ɗaure da sinadarai na halitta yana raguwa a hankali tare da ƙaruwar zafin jiki, yana canzawa zuwa nau'ikan da ke narkewa cikin ruwa, waɗanda za a iya musanya su da ion, ko kuma waɗanda ke ɗaure da carbonate. Wasu vanadium suna amsawa da ma'adanai na calcium da iron don samar da ƙananan abubuwan da ke narkewa.
  • Matakin zafin jiki mai yawa (>1100°C): Sauyin vanadium yana ƙaruwa sosai. Vanadium mai ɗaure da sinadarai yana ruɓewa cikin sauri zuwa nau'in iskar gas mai suna VOₓ (misali, VO, V₂O₅), yayin da vanadium mai ƙarfi (misali, V₂O₃) ya narke kaɗan kuma ya saki ƙaramin adadin vanadium a yanayin zafi mai yawa.
  • Abubuwan da ke tasiri: Yanayin zafi, yawan ƙonewa, da kuma abubuwan da ke cikin ma'adinai suna shafar canjin vanadium. A yanayin zafi mai yawa, vanadium yana samar da tsarin nanocrystalline tare da silicon da sulfur, wanda ke haifar da raguwar volatilization a cikin sigar iskar gas.

3. Hijira da Sauyawar Nickel (Ni)

  • Siffofi na faruwa: Nickel a cikin petroleum coke galibi yana wanzuwa a cikin nau'in sulfide (Ni₃S₂), oxides (NiO2), ko silicates.
  • Matakan ƙarancin zafin jiki (<900°C): Nickel yana wanzuwa a matsayin Ni₃S₂, tare da ƙarancin canjin yanayi.
  • Matsakaicin matakin zafin jiki (900–1200°C): Ni₃S₂ yana canzawa a hankali zuwa NiS a cikin ruwa mai narkewa, yana kaiwa ga kololuwar abun ciki na NiS na kimanin 22.4% a 1200°C, kafin ya koma Ni₃S₂ yayin da zafin ke ƙaruwa.
  • Matakan zafin jiki mai yawa (>1400°C): Nickel yana narkewa a cikin nau'in mahaɗan iskar gas (misali, Ni(g), NiS(g)), amma Ni₃S₂ ba ya canzawa kai tsaye zuwa Ni(s) mai ƙarfi.
  • Abubuwan da ke tasiri: Abubuwan da ke haifar da iskar gas (misali, O₂, H₂O) suna shafar saurin canza nickel. Ƙara O₂ yana hana canza Ni₃S₂ zuwa Ni na elemental kuma yana hana samuwar mahaɗan spinel (misali, NiAl₂O₄).

4. Hijira da Sauyawar Calcium (Ca)

  • Siffofi na faruwa: Calcium a cikin man fetur coke galibi yana samuwa ne a cikin nau'in carbonates (CaCO₃), sulfates (CaSO₄), ko silicates.
  • Matakan ƙarancin zafin jiki (<800°C): Carbonates suna narkewa zuwa CaO da CO₂, yayin da sulfates ke narkewa zuwa CaO da SO₃, wanda ke haifar da wadatar sinadarin calcium a cikin siffa ta oxide.
  • Matsakaicin zafin jiki (800–1200°C): CaO yana yin aiki da silicon da aluminum don samar da ma'adanai masu ƙarancin narkewa (misali, anorthite CaAl₂Si₂O₈), tare da wasu ƙwayoyin calcium da ke cikin siffa mai ƙarfi.
  • Matakin zafin jiki mai yawa (>1200°C): Rashin ƙarfin sinadarin calcium yana da ƙasa, amma ma'adanai masu ƙarancin narkewa na iya narkewa ko ruɓewa a yanayin zafi mai yawa, wanda ke sa sinadarin calcium ya yi ƙaura a cikin iskar gas ko ruwa.
  • Abubuwan da ke tasiri: Yawan sinadarin calcium yana da tasiri sosai ta hanyar rabon silica-alumina da rabon ƙarfe-calcium. Ƙara yawan sinadarin silica-alumina yana haɓaka canza FeV₂O₄ zuwa V₂O₃, yayin da ƙaruwa a cikin rabon ƙarfe-calcium yana hana samuwar CaAl₂Si₂O₈.

Tsarin Cikakkun Bayanai

  • Dogaro da yanayin zafi: Yawan volatilization na abubuwan da aka gano yana ƙaruwa da zafin jiki, amma kewayon zafin volatilization ya bambanta sosai tsakanin abubuwa (misali, vanadium volatilize sosai sama da 1100°C, yayin da nickel ya zama mai mahimmanci sama da 1400°C).
  • Tasirin siffofin faruwa: Abubuwan da ke da alaƙa da kwayoyin halitta (misali, vanadium na halitta) sun fi canzawa fiye da siffofin da ba su da ƙarfi (misali, vanadium oxides).
  • Kula da martanin sinadarai: Ana sarrafa canjin yanayin sinadarai ta hanyar amsawa da sulfur da chlorine, wanda ke samar da ƙananan wuraren narkewa ko mahaɗan iskar gas (misali, Na₂S, VOₓ).
  • Umarnin inganta tsari: Sarrafa zafin calcination, yanayi, da ƙari (misali, masu gyara rabo na silica-alumina) na iya danne yanayin canjin abubuwa masu cutarwa da kuma inganta ingancin calcined coke.

Lokacin Saƙo: Afrilu-17-2026